A blog on the repair, operation and calibration of surface analysis systems and components including electron spectrometers, sputter ion guns and vacuum related hardware. Click on the Index tab below to see a list of all posts. Visit our website at http://www.rbdinstruments.com
Small, inexpensive UHV chambers have been the backbone of many commercial labs and universities for decades. The cost of larger, feature-rich systems has gone up dramatically in recent years, making compact, DIY chambers even more cost-effective for specialized applications and education.
RBD has a range of products available to add value to your compact chamber, and in fact built our own recently to develop and test our microCMA compact Auger analyzer.
We started with an 8 inch spherical octagon chamber from Kimball Physics. This chamber has two 8.00″ CF and eight 2.75″ CF mounts, with an internal volume of 106.6 cu. in. (1,747 cc):
To assist with water vapor desorption, the chamber is fitted with RBD’s miniZ. The mini-Z uses UVC radiation to desorb water from the chamber walls, resulting in faster pump-down times and lower ultimate vacuum.
This chamber is also fitted with RBD’s IG2 2 kV low cost sputter ion gun for specimen cleaning:
The ultimate purpose of this system was to house RBD’s microCMA compact Auger analyzer (shown below with the Z translator attached):
For applications that require elemental analysis, this chamber, with the addition of a PC and CMapp AES acquisition and data massage software, is now a complete system providing quantitative, surface-sensitive Auger electron spectroscopy. At around $50,000 for all the components listed here, this is one example of a budget-sensitive spectroscopy system that can be assembled, repaired and upgraded without costly field service visits.
Our new VB series bakeout packages are an easy way to remove
water vapor from vacuum chambers. The UHV-compatible IRB-600 short wave infrared
radiation emitter mounts on a standard 2.75”/70mm CF flange. The BC-3
controller uses thermocouple feedback to regulate the vacuum chamber
temperature, controls the power to the IRB-600 emitter, and sets the total
bakeout time. These are all the features that you would expect with a vacuum
What sets the VB series BC-3 apart from other bakeout
controllers is the Vacuum Interlock feature. The Vacuum Interlock uses a
Setpoint relay on your vacuum gauge controller to regulate the vacuum level in
the chamber. For example, if your chamber has ion pumps, you can set your
vacuum gauge controller Setpoint to 4 x 10-6 Torr which will turn
off the heat to the chamber when the vacuum setpoint is reached. Whether your chamber has ion pumps or a turbo
pump, the Vacuum Interlock feature can be used to ensure that your pump does
not get choked with water vapor.
The BC-3 controller can drive two IRB-600 emitters, two heater tapes, or even one of each!
Infrared radiation(IR) heats the chamber from the inside out and is very effective compared to external radiant bakeout heaters. The thermal conductivity of stainless steel at 100° C is only 15 W/m K compared to 300 W/m K for copper at 100° C. Therefore, it takes a long time for external bakeout heaters to heat up the inside of the vacuum chamber surfaces.
IR heats the internal surfaces of the vacuum chamber very quickly. Using internal IR heat even for a short time during the initial pump-down can have a noticeable effect on pumpdown times and base vacuum. To reach low UHV vacuum levels you need to bake for longer periods of time.
The short wave IR energy of the IRB-600 emitter drops off as a
function of distance. The internal chamber surfaces that are closer to the
emitter will become hotter than surfaces that are further away from the
emitter. This effect is not precisely linear, but you do need to consider it
with regards to thermocouple sensor placement on the chamber. Typically, the
thermocouple sensor should be about 6-to-10 inches away from the IR-600
emitter. If you have two IRB-600 emitters on your chamber, place the
thermocouple sensor at the midway point between the two emitters.
Once the thermocouple sensor has been placed, you can program
the bakeout temperature setpoint. Typically, the bakeout temperature setpoint
is programed 20° C-to-30° C lower than the temperature on the surfaces that are
nearer to the IRB-600 emitter. If you would like the chamber to be 150° C near
the IRB-600 emitter, program the bakeout temperature to 125° C.
Before using the Vacuum Interlock feature, you need to program
your vacuum gauge setpoint to the desired value. Typically, the vacuum setpoint
is 3 or 4 x10-6 Torr for ion pumps and 5 x 10-4 Torr for
turbo pumps. Then, simply turn the Vacuum Interlock switch on the BC-3
controller to On. If you would prefer to bake the chamber into the turbo pump
before you turn on your vacuum gauge, then set the vacuum interlock switch to
Off; the IRB-600 emitters will turn on and be regulated only by the vacuum
In our shop we have a few vacuum chambers that come up to air practically every day, and some days more than once per day. We use the BC-3 with a single IRB-600 emitter and one 600 watt heating tape to effectively remove water vapor. If we know that we will be venting again later in the day, we turn on the BC-3 as soon as we start pumping down the chamber in order to take advantage of viscous flow and to let the turbo pump down the chamber for about 30 minutes. Then we turn off the BC-3 and start the ion pumps; the vacuum chamber will be down in the low 10-8 Torr range within a few hours. If we need a better vacuum, then we bake the chamber out for 8-to-10 hours over night. The following day the vacuum chamber will be in the 10-10 Torr range after the chamber cools down and also using a titanium sublimation pump. Not needing to remove cables and preamplifiers from the chamber is a big time-saver. We use the VB bakeout package practically every day and every time we do, we really appreciate how easy it is to bakeout a vacuum chamber with the BC-3 and IRB-600 compared to external heaters and bakeout blankets.
The BC-3 and IRB-600 are available in 120 VAC and 230 VAC configurations.
For more information on the VB series bakeout controller, visit
our website at this link –