72-100 voltage

I recently encountered an unusual problem on two different 660 scanning auger systems within a period of a few months where the 72-100 multiplier voltage would drop off after a period of time.

On one system the 97 SED preamp would fail after a few minutes of warm up time, resulting in no image. On the other system the 96A V/F preamplifier would fail after 20 to 30 minutes, resulting in no AES data.

In both cases I measured the multiplier supply voltages at the preamp and the voltages were there when functioning and not there or unstable when in the failed mode. So easy enough, that should be a problem on the 72-100 board. To verify that the problem was on the board I swapped the 72-100 board with the other one. For those of you not familiar with the 660 scanning auger system or the 72-100 electron multiplier supply, there are two 72-100s on a 660. One is for the CMA AES analyzer and the other one is for the 97 SED preamplifier. The boards are identical and can be swapped out by physically moving the boards and changing an address switch.

Swapping the 72-100 boards produced the same result. That meant that the problem was not on the board, so the next most likely thing was the SHV multiplier supply cable. Those cables checked out fine with an ohmmeter but to be sure I also swapped the cables out and the problem was still there.

So as unlikely as it was, the only thing left was the 72-100 mother board.   I pulled out the mother board looking for a bent pin or something that could explain the problem and did in fact find that one of the 1K ohm filter resistors was out of spec and looked like it had been running hot. Moving it slightly caused the resistor to break in two.

Here is a picture of the motherboard that shows the resistor:

72-100 R1 R2

72-100 R1 R2

And here is the schematic that shows both resistors:

72-100 mother board schematic

72-100 mother board schematic

Replacing the defective resistor solved the problem. What was interesting for me with this problem was that in over 37 years of working with PHI surface analysis systems I had never seen this problem before, and then I saw the same problem on two different systems within a short period of time.

If you have an intermittent SED image or AES data problem on your 660 (or 4000 series) scanning auger system, keep this solution in mind as something to check.

10-155 Filament replacement procedure

This blog post is an updated version of the 10-155 filament replacement procedure first published on the RBD Instruments website as a Technical Tip a number of years ago. This version has been updated with some close up pictures of the electron gun assembly shown at the bottom of this post.

Use gloves, de-magnetize all tools and clean all tools with Isopropanol.

  1. Set analyzer on stand or use manuals and support analyzer on handles, facing up.
  2. Remove outer magnetic shield (4 screws)
  3. Remove inner magnetic shield (4 screws)
  4. Carefully remove conical ceramic
  5. Loosen VM (outer cylinder) wire and lift inner cylinder off of base ceramic.
  6. Remove 3 screws inside inner cylinder.
  7. Carefully lift inner cylinder up and off of the electron gun assembly. Note: If the inner cylinder does not move freely, use a heat gun to expand the inner cylinder so that it will slide off. Do not force it!
  8. Look at the 10-155 electron gun detail PDF file to familiarize yourself with the electron gun assembly.
  9. Remove the three long screws that hold the electron gun assembly together.
  10. Remove the V1 emission screw
  11. Remove the 2 filament couplers from the filament posts. You will need a .048 4 spline wrench.
  12. Remove the 3 filament ceramics.
  13. Remove the filament assembly. Note the orientation of the emission tab and filament posts.
  14. Remove the 3 screws that hold the filament base on and remove the filament.
  15. Install the new filament in the same orientation as the old filament into the emission cap.
  16. Install the 3 screws and the filament base and tighten slightly.
  17. Position the filament so that it is centered in the hole and tighten the 3 screws. This is best done using a microscope.
  18. Install the filament assembly on top of the 3 filament ceramics and use the 3 long screws to hold the assembly together. The three long screws need to be tightened so that they all have the same distance with respect to the base.
  19. Reconnect the V1 wire
  20. Reconnect the filament couplers.
  21. Ohm out the connections to the filament and V1.
  22. Degauss the gun assembly.
  23. Install the inner cylinder over the electron gun assembly.
  24. Reinsert and tighten the three screws inside the inner cylinder.
  25. Reinstall the outer cylinder and attach the VM wire.
  26. Carefully install the conical ceramic. The resistor part should be 180 degrees out from the bottom flat ceramic. Ohm out VM to ground and make sure it has the correct resistance – typically that is about 3 Meg ohms from VM (the outer cylinder) to ground. You may need to shim the inner or outer cylinder with some silver or platinum foil, see the 10-155 shim document for more information. Both the flat and conical termination ceramics need to make a good electrical connection in order for the CMA to properly focus the electrons into the analyzer aperture.
  27. Install the inner magnetic shield
  28. Degauss the analyzer.
  29. Install the outer magnetic shield.
  30. Degauss the analyzer. Installation complete!

RBD Instruments provides the C75-010 filament and electron multiplier used in the 10-155 CMA. Contact us for more information.

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