Ion pump elements – Flip the plates part II

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Our previous blog post explained how to flip the ion pump Tantalum and Titanium plates in order to provide fresh surface area for the sputtering process that occurs as part of the ionization / pumping process.

But what happens if you flip the plates and then years later the ion pumps are worn out again? That is, what if both sides of the plates have been sputtered?

This blog post will explain how you can modify the plates to expose a fresh surface area which functionally is the same thing as replacing the plates.

Like most things, ion pump elements have gone up in price post COVID.  A set of 8 elements (there are 8 elements in a 220 l/s ion pump) can cost $5,000 or more.    Rather than replacing the elements, you can replace just the ceramics for a lot less and flip the plates.   If the plates have already been flipped once, then both sides of the plates will have sputtered craters. 

By elongating the mounting holes in the plates by 1.5 mm the sputter area on the plates would also shift by 1.5 mm onto a fresh area that has not been sputtered, at least not sputtered very much.

The photos below show the sputtered craters and the location of where the new sputtering will occur.

Sputtered crater
Sputtered crater
Offset by 1.5mm
Offset by 1.5mm
elongated hole
Elongated hole
new sputter area
new sputter area

In this case I was lucky enough to be at a university with a machine shop and the machinist was able to punch the holes without using any oil.  If you do not have a machine shop, you could use a Dremel cutting bit to elongate the holes.

dremel cutting bit

When you reassemble the elements, you want to make sure that you offset both the Tantalum and the Titanium plates in the same direction.  You will be able to tell that the Tantalum plate is offset by the 1.5mm gap with respect to the stainless-steel backing plate.  Then make sure that the Titanium plate lines up with the location of the Tantalum plate.  You can confirm that the Titanium plate is offset correctly by looking at the distance on the mounting tabs on the back of the Titanium plate.

Titanium plate offset
Titanium plate offset

After performing this procedure on the plates shown in this blog post the ion pump elements performed as well as new elements.  The increase in pumping capacity was noticeable.

If you suspect that your ion pumps may need to be inspected (slow pumping, arcing, or shorted) I recommend that you buy the ion pump ceramics before you vent so that you have them on hand if needed.  RBD Instruments provides ion pump ceramics.  Contact us for more information.

Scientific Glassblowing Resources

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Glassblowing has been around for thousands of years, and we see examples of it every day. From neon signs to Murano glass to Chihuly glass exhibits. Less well known but very important to science is the art and craft of scientific glassblowing which is the process of creating glass apparatus used in research and production.

Over the years I have had the good luck to be working at universities on one or another type of vacuum chamber related instrument where some glass to metal seal was damaged but was able to be repaired by the resident glass blower.  More recently it seems that many of the glassblowers at universities are retiring and not being replaced. So, to an extent, scientific glass blowing is becoming a nearly lost art as this interesting article on the History of Glassblowing explains.

But all is not lost as there are still scientific glass blowers who are handing down their glassblowing expertise to those who will carry on the tradition.

Also, there are some schools which offer glassblowing courses such as Salem Community College.

Listed below are some companies that provide custom scientific glass blowing services. These companies can also repair broken glass to metal seals.

Nunn Better Glass

http://www.nunnbetterglass.com/

Precision Glass Blowing

https://www.allenglass.com/

https://farlowsci.com/

Finally, The American Glassblowers Society has a Find a Glassblower link that lists glass blowers from different parts of the USA. https://asgs-glass.org/#

Electron multipliers for older PHI AES and XPS systems

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4831G Channeltron Electron Multiplier

The original channeltron and channel plate electron multipliers for the older PHI (Physical Electronics) AES and XPS systems are still available through Photonis.  The cost of these parts has increased substantially in the last few years, so be prepared for sticker shock the next time you need a channeltron or a set of channel plates!

Here are the Photonis part numbers for the different PHI systems:

Model NumberWhere usedPhotonis Part Number
4831G15-255G, 25-120, 25-120A, 25-130, 25-270 and 25-260 cylindrical mirror analyzers. 06-600 SIMS, 590 through 660 scanning AES systems30129
483910-150 and 10-155 CMA30131
48215100, 5300 and 5400 XPS systems 10-360 SCA single channel detector30117
PSD detector channel plate matched set EDR5400 XPS system 10-360 SCA PSD  position sensitive detector30300
MCD chevron plate set EDR5500 through 5800 XPS 10-360 SCA MCD 16 channel detector30410

For a quotation you can call 1-508-347-4000 or request a quotation at this URL –

https://www.photonis.com/products/microchannel-plates